全自動定氮儀洗滌過程尤為關鍵
全自動定氮儀作為蛋白質含量檢測的常用設備,如今在很多食品檢測部門都能看到它的“身影”。儀器的外觀看起來雖然簡單,但實際是“深藏不漏”,它ta的de操cao作zuo要yao求qiu較jiao高gao,使shi用yong過guo程cheng中zhong的de每mei一yi步bu都dou可ke能neng會hui影ying響xiang最zui終zhong的de測ce量liang結jie果guo,特te別bie是shi設she備bei的de洗xi滌di過guo程cheng尤you為wei關guan鍵jian,大da部bu分fen的de儀yi器qi都dou需xu要yao按an照zhao以yi下xia方fang法fa正zheng確que洗xi滌di。
安裝前,各部件需經一般方法洗滌幹淨,所用橡皮管、塞須浸在10%氫氧化鈉溶液中,煮個大約十分鍾,水洗、水煮也得十分鍾,然後安裝並固定在一隻鐵架台上。

shiyongqian,quanzidongdingdanyidequanbuguandaodouxujingshuizhengqixidi,yichuquguandaoneikenengcanliudean,zhengzaishiyongdeyiqi,meiciceyangqian,zhengqixidiwufenzhongjike。jiaochangshijianweishiyongdeyiqi,zhongfuzhengqixidi,budeshaoyusanci,bingjianzhayiqishifouzhengchang。zaixijianzhagegelianjiechu,baozhengbulouqi。 首先在蒸氣發生器中加約2/3體積蒸餾水,加入數滴硫酸使其保持酸性,以避免水中的氨被蒸出而影響結果,並放入少許沸石,以防爆沸。沿小玻杯壁加入蒸餾水約20毫(hao)升(sheng)讓(rang)水(shui)經(jing)插(cha)管(guan)流(liu)入(ru)反(fan)應(ying)室(shi),但(dan)玻(bo)杯(bei)內(nei)的(de)水(shui)不(bu)要(yao)放(fang)完(wan),塞(sai)上(shang)棒(bang)狀(zhuang)玻(bo)塞(sai),保(bao)持(chi)水(shui)封(feng),防(fang)止(zhi)漏(lou)氣(qi)。蒸(zheng)氣(qi)發(fa)生(sheng)後(hou),立(li)即(ji)關(guan)閉(bi)廢(fei)液(ye)排(pai)放(fang)管(guan)上(shang)的(de)開(kai)關(guan),使(shi)蒸(zheng)氣(qi)隻(zhi)能(neng)進(jin)入(ru)反(fan)應(ying)室(shi),導(dao)致(zhi)反(fan)應(ying)室(shi)內(nei)的(de)水(shui)迅(xun)速(su)沸(fei)騰(teng),蒸(zheng)出(chu)蒸(zheng)氣(qi)由(you)反(fan)應(ying)室(shi)上(shang)端(duan)口(kou)通(tong)過(guo)定(ding)氮(dan)球(qiu)進(jin)入(ru)冷(leng)凝(ning)管(guan)冷(leng)卻(que),在(zai)冷(leng)凝(ning)管(guan)下(xia)端(duan)放(fang)置(zhi)一(yi)個(ge)錐(zhui)形(xing)瓶(ping)接(jie)收(shou)冷(leng)凝(ning)水(shui)。從(cong)定(ding)氮(dan)球(qiu)發(fa)燙(tang)開(kai)始(shi)計(ji)時(shi),連(lian)續(xu)蒸(zheng)煮(zhu)五(wu)分(fen)鍾(zhong),然(ran)後(hou)移(yi)開(kai)煤(mei)氣(qi)燈(deng)。衝(chong)洗(xi)完(wan)畢(bi),夾(jia)緊(jin)蒸(zheng)氣(qi)發(fa)生(sheng)器(qi)與(yu)收(shou)集(ji)器(qi)之(zhi)間(jian)的(de)連(lian)接(jie)橡(xiang)膠(jiao)管(guan),由(you)於(yu)氣(qi)體(ti)冷(leng)卻(que)壓(ya)力(li)降(jiang)低(di),反(fan)應(ying)室(shi)內(nei)廢(fei)液(ye)就(jiu)會(hui)自(zi)動(dong)抽(chou)到(dao)反(fan)應(ying)室(shi)外(wai)殼(ke)中(zhong),打(da)開(kai)廢(fei)液(ye)排(pai)出(chu)口(kou)夾(jia)子(zi)放(fang)出(chu)廢(fei)液(ye)即(ji)可(ke)。這(zhe)樣(yang)清(qing)洗(xi)2~3ci,ranhouzailengningguanxiafangyigeshengyoupengsuanzhishijihunheyedezhuixingpingshilengningguanxiakouwanquanjinmeizairongyezhong,zhengliuliangfenzhong,guanchazhuixingpingneiderongyeshifoubianse。rububianse,biaoshizhengliuzhuangzhineibuyixiganjing,yiquzhuixingping,zaizhengliuliangfenzhong,yongzhengliushuichongxilengningqixiakou,guanbimeiqideng,zhenggexidiguochengwancheng,quanzidongdingdanyifangkegongceyangpinshiyong。



