KDN係列凱氏定氮儀最新操作方法
KDN係列凱氏定氮儀shiceliangdanhanliangdezuichangyongyiqi,genjujingdiandekaishidingdanfayanzhi,jingguozhemeduonian,yiqiyeyoulegengxindiedai。weilefangbiandajiashunlikaizhanshiyan,xiaobianweidajiazhenglileyifenzuixindekaishidingdanyicaozuofangfa。

1. 儀器安裝
jiangpeijianzhongdeguijiaoguangenjushijixuqiujianchengbutongdechangdu,bingqielianjiehao。zhengliushuijinkouhejianyejinkoudeguijiaoguanlingyiduanbixujinpaozaisuoduiyingdeyemianyixia。zhengliushuichukouhelengqueshuichukoudeguijiaoguanlingyiduanfangrupaishuichi。lengqueshuijinkoulianjiezilaishuilongtou。zaiyiqizhengmianzuocetuopanshanganfangkongdexiaohuaguan,youcefangzhuixingping,charudaixiangpisaidebolizui。
2. 儀器檢測
(1)打開水龍頭開關,注意流量,控製在3-4L/fenzhong。jieshangdianyuanxian,dakaidianyuanzongkaiguan。yiqikaishizidongjiashui,congcemianshaobeishuiweiguancekoukeyikanjianshaobeineideshuiweishangsheng,yiduanshijianhouhuizidongtingzhijiashui。
(2)打開加堿按鈕,加堿量大概在30mL左右時,關閉加堿按鈕。接著打開蒸餾按鈕,儀器開始蒸餾。儀器工作10分鍾左右,關閉蒸餾按鈕,儀器停止蒸餾,整機檢測完成。
3. 實驗蒸餾
在zai消xiao化hua管guan托tuo盤pan上shang換huan上shang已yi消xiao化hua完wan成cheng並bing冷leng卻que稀xi釋shi後hou的de樣yang品pin,右you側ce換huan成cheng準zhun備bei好hao的de錐zhui形xing瓶ping,調tiao整zheng氨an氣qi回hui流liu玻bo璃li嘴zui和he瓶ping塞sai,使shi玻bo璃li嘴zui浸jin泡pao在zai硼peng酸suan液ye麵mian以yi下xia。然ran後hou先xian打da開kai加jia堿jian按an鈕niu,加jia到dao自zi己ji所suo需xu要yao的de堿jian的de用yong量liang後hou,關guan閉bi加jia堿jian按an鈕niu。然ran後hou再zai打da開kai蒸zheng餾liu按an鈕niu。蒸zheng餾liu即ji將jiang完wan成cheng後hou,提ti起qi橡xiang皮pi塞sai,移yi開kai錐zhui形xing瓶ping,使shi氨an氣qi回hui流liu玻bo璃li嘴zui離li開kai液ye麵mian,用yong蒸zheng餾liu水shui衝chong洗xi玻bo璃li嘴zui外wai壁bi,繼ji續xu蒸zheng餾liu10秒鍾後,關閉蒸餾按鈕,取下錐形瓶待滴定、計算。



